WebSynthesis of (3,3-Dimethoxyprop-1-enyl)benzene (2) To a solution of cinnamaldehyde (6.6 g, 0.05 mol) in 60 mL dried methanol, trimethyl orthoformate 20.0 g (0.188 mol) and 30 mg (0.015 mmol) p -toluenesulfonic acid monohydrate was added with a stirrer bar under nitrogen atmosphere. WebCinnamaldehyde is the main component in cinnamon oil, which is extracted from cinnamon by steam distillation. As an important spice and organic intermediate, it is widely used in ... organic synthesis and oxidation mechanism of cinnamaldehyde. Materials and experimental procedures Materials Cinnamaldehyde (99%, Shanghai Medical Technology Co.,
a wittig reaction of trans-cinnamaldehyde lab report - Example
WebSep 30, 2014 · Cinnamaldehyde, the bioactive component of the spice cinnamon, and its derivatives have been shown to possess anti-cancer activity against various cancer cell … WebThe synthesis of trans-cinnamaldehyde by using the aldol reaction of benzaldehyde and acetaldehyde. Also, the base-catalyzed aldol reaction is explained and why trans-cinnamaldehyde is the major ... sundoo townsville
CN105152891A - Synthesis method of cinnamaldehyde
WebApr 1, 2024 · The hydrogenation of cinnamaldehyde was carried on a autoclave reactor (Anhui Kemi Machinery Technology Co., LTD, China). In typical, a 3 mg catalyst was mixed into the reactor with 0.2 mmol of cinnamaldehyde. Methanol, ethanol, and deionized water were used as the solvent, respectively. WebCinnamaldehyde tosylhydrazone Mix 130ml of Cinnamaldehyde and 260ml of 95% ethanol in a 1L RB flask equipped with a reflux condenser. Then add 220g of p -toluenesulfonylhydrazide. Swirl the contents of the flask. Heat the flask at 100°C with magnetic stirring (or stirring of some kind). WebCinnamaldehyde is converted into HC through the synthesis design in three-reaction steps, including nitration using nitric acid-acetic acid anhydride at 0-5 °C, reduction in mild condition by ... sundown allentown